National Physical Laboratory

Testing services

Corrosion

  • Testing in H2S environments
    • dedicated test laboratory
  • Materials selection for resistance to environment assisted cracking
    • proof rings, 4 pt bend, C-rings; slow strain rate and corrosion fatigue, HIC
    • drop-evaporation SCC kit
    • hydrogen permeation test systems to measure hydrogen uptake and diffusion rate
  • 8 autoclaves for high pressure/high temperature testing
  • Corrosion inhibition measurement
    • small-scale flow loop
    • multi-electrode underdeposit corrosion facility
  • Pitting, crevice and intergranular corrosion evaluation
    • crevice assemblies
    • galvanic corrosion testing
    • electro-potential reactivation test for intergranular corrosion in sensitized alloys and for depleted zones associated with particles (e.g. s-phase in DSS)
    • critical pitting temperature
    • pitting and repassivation potentials
    • potentiodynamic test stations
    • scanning electrochemical microscopy
  • Electrochemical impedance spectroscopy
  • Failure analysis
  • Corrosion consultancy

Photovoltaics and Organic Electronics

  • Opto-electrical measurements
    • Display metrology
    • Electro-absorption: built-in electric field
    • Dark injection transient spectroscopy: charge mobility
    • Probe station with inert atmosphere and variable temperature linked to semiconductor parameter analyzer
    • Class AAA solar simulator: solar cell efficiency
    • Current vs. voltage measurements (in dark or under simulated sun light)
    • IPCE/EQE - Incident photon-to-current conversion efficiency (external quantum efficiency): spectral photoresponse for solar cell characterization
    • Micro to millimeter scale photocurrent mapping (up to 225 cm2 samples) (LBIC, broadband illumination)
    • Electrical characterisation of interconnects

Electrochemical Testing and Imaging

  • Potentiostatic/potentiodynamic polarisation
  • Rotating disc/cylinder electrode systems
  • Scanning electrochemical microscopy (SECM)
  • Scanning ion conductance microscopy (SICM)
  • Scanning vibrating electrode system (SVET)
  • Electrochemical impedance spectroscopy (EIS)

Fuel cells

  • Single cell and short stack testing up to 500 W (PEMFC)
  • Instrumented single cell testing - in situ measurement of potential, humidity, temperature, localised current density
  • Corrosion testing of metallic bipolar plates
  • Electrochemical characterisation of fuel cell electrocatalysts

Material Characterisation

  • Scanning probe microscopies
    • AFM - Atomic force microscopy: topography
    • SKPM - Scanning Kelvin probe microscopy (atmospheric and ultra-high vacuum): workfunction
    • C-AFM - Conductive AFM: nanoscale current response
  • Surface analysis
    • XPS - X-ray photoelectron spectroscopy: surface chemical composition
    • UPS - Ultraviolet photoelectron spectroscopy: material workfunction
    • TOF-SIMS – Time of flight secondary ion mass spectrometry: chemical depth profiling
    • Contact angle measurement: surface energy mapping for print deposition characterisation
    • Spectroscopic ellipsometry: film thickness and optical properties
  • Morphological characterisation
    • Scanning Electron Microscopy (SEM) with EDX and WDX analysis
    • Field emission SEM: high-resolution images of nanoscale topographic features
    • Electron back-scattering diffraction (EBSD)
    • Confocal and optical microscopy: surface topography
    • White-light interferometry: surface roughness, topography
  • Mechanical characterisation
    • Nano-indentation: modulus, creep, hardness and impact properties
  • Rheology