National Physical Laboratory

Contamination

Radiation Sign

A contamination monitor calibration certificate records the instrument’s response to a range of International Standards Organisation (ISO) reference sources at a specified distance.

These are a set of specialist sources produced for the purpose of calibration which are designed to provide calibration laboratories with a consistent, reproducible method of determining a detector’s response to a range of radiation types and energies.

The traceable quantity of a reference source is the surface emission rate per unit area (SER) which is the number of particles or photons emitted from the surface of the source per second.

Instrument testing/calibration should be carried out in accordance with NPL good practice guides 14 and 29.

The results of a calibration of a surface contamination monitor may be quoted on a certificate in various ways:

IR(E): Response in terms of emissions per unit area

radiationFormula

where Ri is the observed reading (s-1)

            B is the background count rate (s-1)

SER is the surface emission rate per unit area (α, β or photon) s-1cm-2

E.g. If an instrument reading of 80 βs-1 were obtained on exposure to a 36Cl reference source of emission rate 25 β s-1 cm-2

radiationFormula

This is the response to beta radiations of maximum energy 708 keV in terms of surface emission rate.



2π eff: Efficiency in terms of SER

 radiationFormula

E.g. Using the example above and where Ap = probe area (10 cm2 in this example)

radiationFormula

This is the efficiency to beta radiations of maximum energy 708 keV  in terms of surface emission rate.

Or

CFE: Calibration factor in terms of SER.  Note CFE is the reciprocal of IR(E)

 radiationFormula                                 radiationFormula

This is the calibration factor for 36Cl. The net instrument reading should be multiplied by this to obtain the number of beta particles detected per unit area.

Or

IR(A): Instrument response  in terms of activity

The calibration laboratory may provide the instrument’s response to the source activity. For the calibration sources involved, in a controlled environment, this is relatively easy to estimate

radiationFormula

Where P = P-factor and describes the relationship between the particle or photon generation rate and the emission rate from the surface.36Cl has a P factor of 2 because there is a simple relationship between the number of beta emissions that emerge (SER) and the source activity. Other radionuclides may have more complicated decay schemes, further guidance on this can be found in the module ‘estimating surface activity’

E.g. 36Cl response {for an ideal source of 36Cl, P=2}

radiationFormula

This is the response to beta radiations of max energy 708 keV in terms of activity.
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