National Physical Laboratory

Minutes of the Third GSUF Meeting

27 November 2000

National Physical Laboratory

 

Participants:     Fiona Barr British Energy, Hunterston B
    Michel Ceuppens Canberra Packard, Belgium
    Peter Danyluk AWE Aldermaston
    Julian Dean NPL
    Tony Dell VLA
    Jim Desmond BNFL Geoffrey Schofield Laboratories
    Mike Dolan AWE Aldermaston
    Steve Dunkley Harwell Instruments
    Trevor Hatt Perkin Elmer
    Elizabeth Howie British Energy, Hunterston B
    Simon Jerome NPL
    Satwant Johal NPL
    Elisabeth Jones University Hospital of Wales
    Steven Judge AEA Technology QSA
    John Lees BNFL Magnox
    Andrea Lewis NNC WQCL
    Richard Lukey VLA
    Bob Major NNC
    John Makepeace NPL (Chairman)
    Fiona Miller UKAEA Dounreay
    Andy Pearce NPL
    Martin Phillips BNFL Berkeley
    Calvert Pratt BNFL Berkeley
    Anne Ross UKAEA Dounreay
    Martin Rushby AWE Aldermaston
    Bob Sharrock Urenco
    Matthew Simpson DERA RPS
    Robin Treadwell AWE Aldermaston
    Tim Twomey Perkin Elmer
    Stephanie Vallet Harwell Instruments
    Doug Van Cleef Perkin Elmer
    Steve Waters MRC Clinical Sciences Centre
    Mike Woods NPL
    Simon Woods NPL (Secretary)
    Mike Youngman NRPB

1. Chairman’s opening remarks

The Chairman welcomed those present. He noted that this was an extraordinary meeting of the forum in that NMSPU funding only covered two meetings of the GSUF. In the forthcoming new three year programme, annual meetings were planned.

2. Minutes of the 2nd meeting – 29 October 1999

These were accepted without correction.

3. Matters arising from the minutes

Action 2.1: Simon Woods/Ian Adsley to discuss (use of AEAT decay data) with interested parties to agree a suitable format.

Discussions ensued as to the suitability of this approach. Opinion was split between users’ with some not wanting an alterable database whilst others preferred an easy load format. Mike Woods commented that there needs to be one agreed data set and that it should be agreed internationally. The current evaluation work being undertaken by an IAEA CRP will be accepted as authorative, but it comprises a limited set of data.

The Radiochemical Manual data itself is “owned” by AEA Technology with funding provided from the DTI through NMSPU. If this data were to be used, the legality of such a step would have to be checked with both parties.

Further discussion of nuclear decay data was deferred to later on the agenda.

Action 2.1a: All: Inform Simon Woods of any Millenium Compliance problems experienced for dissemination.

No problems reported. Action completed.

Action 2.2: NPL (Simon Woods) to devise and distribute a questionnaire on user requirements for intercomparisons.

Action 2.3: NPL (Simon Woods) to devise and distribute questionnaire to determine problems with low energy gamma-ray measurements.

These actions were deferred to later in the agenda.

Action 2.4: All to send any comments on the (MDA) subgroup proposals to Simon Woods by end of December.

Only one response has been received. Results of the working group will be redistributed with the current minutes to stimulate discussion. It was suggested that participants in the environmental intercomparison be asked to report MDAs. For the MDAs, participants should not be worried about the slight difference between 95% CL and k=2.


Action 2.5: NPL (Simon Woods) to gauge amount of interest in proposed meetings (with manufacturers), which manufacturers to target and identify topics for discussion.

Harwell Instruments and EG&G both present at the forum and had agreed to give presentations (see later).

Action 2.6: All to submit any data they may have on this (226Ra 186 keV) transition to Simon Woods.

Two user responses received. Simon Woods will give a short presentation on the apparent resolution of the problem later in the forum.

Action 2.7: NPL (John Makepeace) to investigate the possible funding of a third meeting of the GSUF within the current NMSPU Ionising Radiation programme.

This forum. NMSPU have agreed to the principle that the minimum should be at least once a year. Action completed.

4. User discussion

4.1 226Ra

Simon Woods gave a short presentation detailing a new measurement of the alpha branching ratios reported at the MARC V conference in Hawaii. From these data, a gamma-ray emission probability for the 186 keV transition of 0.0364(4) may be derived, in agreement with directly determined values (which previously deviated by 9% from values derived from decay scheme balances).

It was noted that Alan Nichols (Harwell) was in the process of undertaking a re-evaluation of this radionuclide as part of the Decay Data Evaluation Project. This new evaluation will be public domain.

4.2 Propagation of uncertainties in detection limits

Many users consider only statistical uncertainties and ignore any systematic components. An accepted method of propagation needs to be defined.

Michel Ceuppens (Canberra Packard, Belgium) informed the forum that their software takes systematic uncertainties from the efficiency curve, but uncertainties in positioning and density are not taken into account. Consequently, a user will need to increase any reported MDA, estimated from the sample background, to compensate for this.

In a similar vein, Doug van Cleef (Perkin Elmer, USA) commented that the principal component to an MDA is the background uncertainty. If numerous measurements of blanks are taken, this will include uncertainties, such as positioning, in an empirical manner. A single measurement is not ideal. Other uncertainties may be propagated by normal methods.

NPL does run courses on uncertainties. What most users require is a body to examine, identify and quantify all uncertainties, with national laboratories disseminating the methods. It was suggested that a sub-meeting of the GSUF be held to consider this topic.

Interested members:   Bob Sharrock
  Matthew Simpson
  Richard Lukey
  Steve Judge
  Mike Youngman
  Tony Ware
  Bob Major

Tony Ware commented that the Chemistry Commission has also raised this topic.

4.3 ISO 9000:2000

The forum members were generally happy with this accreditation system. The majority of those present were covered for QA; 1/3 through ISO and 2/3 through UKAS.

4.4 Questionnaires

Members of the forum suggested a number of additions to the questionnaires relating to actions 2.2 and 2.3. These suggestions will be incorporated into the documents and the forms distributed to all interested parties, preferably as Word 6 documents.

Action 3.1: NPL (Simon Woods) to amend and distribute questionnaires.

4.5 Radionuclide decay data libraries

It was suggested that a “cut and paste” format could be the way forward, but some participants were worried about validating such a format. There needs to be fields to identify references and alteration dates. The manufacturers present indicated that they were amenable to this idea.

There is a strong requirement for an international body to agree upon a data set. It was suggested that an appropriate assembly might be ICRM.

5. Manufacturers’ presentations

5.1 Michel Ceuppens (Canberra Packard)

Topics: Genie 2000 v2.0
  TCS theory
  ISOCS/LABSOCS
  Traceability

5.2 Doug van Cleef / Tim Twomey (Perkin Elmer)

Topics: X-Cooler
  Detector configurations
  DigiDART
  SMART 1 HPGe
  GammaVision 5.2
  Isotopic

6. Concluding discussions

It was noted that the IRMF maintain a register of people providing services, primarily commercial but also internal. It was felt that the GSUF should follow this route.

Action 3.2: NPL (Simon Woods) to devise and distribute a suitable questionnaire

It was noted that information would only be made available for dissemination with the express permission of the service provider.

 

Simon Woods

Secretary, GSUF

Last Updated: 24 May 2010
Created: 24 May 2010